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In this study, the effect of firing temperatures on phase formation, microstructure dielectric and magnetic properties of Ni 0.6 Zn 0.4 Fe 2 O 4  (NZFO) ceramics were investigated. The NZFO powder were synthesized by the solid-state combustion technique using glycine as a fuel to reduce the reaction temperature. All samples were calcined in the range of 900 °C–1100 °C for 2 h and sintered in the range of 1175 °C–1275 °C for 2 h. A pure ferrite phase was found in the powders calcined above 1000 °C and the average particle size of NZFO powders was increased from 0.39  µ m to 0.59  µ m when the calcination temperature was increased. The x-ray diffraction (XRD) analysis results confirmed the formation of pure spinel structure with cubic phase in all the ceramic samples. The average grain size (5.54–2.80  µ m) was slightly decreased, and the dielectric constant (239–13) tended to decrease with increasing sintering temperature. As the sintering temperature increased to 1250 °C, it was found that the lattice parameters (8.366–8.387 Å), the density (5.29–5.35 g/cm 3 ), and saturation magnetization (81.51–93.92 emu/g) tended to increase after that decrease.

integrated ferroelectrics

Effect of Firing Temperatures on Phase Formation, Microstructure, Dielectric and Magnetic Properties of Ni 0.6 Zn 0.4 Fe 2 O 4  Ceramics Synthesized by the Solid-State Combustion Technique