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The Chalcopyrite CuInS 2  films were prepared from nitrates below 220 °C. When the anhydrous ethanol is used as the solvent, the reaction cycle, temperature and holding time are main factors affecting crystallization. Increasing the reaction cycle, temperature and holding time are beneficial to the crystallinity. CuInS 2  films prepared with thioacetamide and thiourea as sulfur sources have the chalcopyrite structure, the crystallinity of CuInS 2  film prepared by thiourea is slightly better than that of by thioacetamide. It consists of spherical particles with diameters of 0.1 ∼ 0.4 μm. The band estimated gap of chalcopyrite CuInS 2  film samples is about 1.49 ∼ 1.51 eV.

Systematic Study on Preparation of CuInS 2 Films with Chalcopyrite from Nitrates