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A composite from a ferroelectric metal–organic framework of [ND 4 ][Zn(DCOO) 3 ] and nano-dispersed silicon dioxides nanoparticles (nSiO 2 ) has been synthesized. The study investigates the influence of nSiO 2  on ferroelectric switching and phase transition properties in [ND 4 ][Zn(DCOO) 3 ]. It was indicated that the addition of nSiO 2  led to the increase in phase transition temperatures and the inhibition of repolarization in ferroelectric parts. When the nSiO 2  amount increased, the saturated dielectric hysteresis loops were more difficult to obtain and transformed into unsaturated ones with the rise of coercive field. The residual water molecules kept on nSiO 2  were found to be responsible for the above anomalies.

Ferroelectric Switching and Phase Transition in Composites from Ferroelectric Metal–Organic Framework of [ND 4 ][Zn(DCOO) 3 ] and Silicon Dioxides