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The synthesis of CpFe(CO) 2 ECOCH 2 CO 2 R [E = S ( 1 ), Se ( 2 ); R = Me ( a ), Et ( b )] was achieved by treating (µ-Ex)[CpFe(CO) 2 ] 2  (E = S,  x  = 2–4, Se,  x  = 1) with alkyl malonyl chlorides at ambient temperature. The synthesized compounds were characterized by elemental analysis, FT-IR,  1 H and  13 C NMR spectroscopy as well as with UV–Vis spectroscopic techniques. The molecular structures of  1a  and  2a  were determined by single crystal X-ray diffraction studies and reveal that the two compounds are monomeric in the solid state with the iron center located in a distorted octahedral environment.

Synthesis, spectral and structural characterization of iron chalcogenomalonato complexes CpFe(CO) 2 ECOCH 2 CO 2 R (E = S, Se)