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An ultrasound-assisted simple, easy and straightforward method for the synthesis of α-aminophosphonates has been developed  via  Kornblum/Kabachnik-fields reaction. The method involves  in situ  generation of an aldehyde intermediate from benzyl halides  via  oxidative dehalogenation followed by coupling with aryl amine and trialkyl phosphite in a one-pot three component manner under ultrasonic irradiations. The developed method is compatible with various functionalities and the desired products are obtained in good to excellent yield under mild conditions.

An ultra-sound assisted synthesis of α-aminophosphonates from benzyl halides via sequential Kornblum and Kabachnik-fields reaction