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A series of MoP catalysts (MoP-CA x ) were synthesized by adding citric acid (CA) to solutions of (NH 4 ) 6 Mo 7 O 24 ·4H 2 O and (NH 4 ) 2 HPO 4  with a fixed molar ratio of Mo:P:CA = 1:1:  x  ( x  = 0, 1, 4, 8) followed by drying and reduction in H 2 . The addition of CA had a significant effect on the microstructure (surface area and particle dispersion) and performance of MoP for dry reforming of methane (DRM). Among these MoP-CA x  catalysts, the MoP-CA8 was found to show the highest catalyst stability, which should be attributed to the best matching of oxidation resistance ability and methane dissociation ability of MoP.

The effect of citric acid on the microstructure and activity of MoP phosphide for dry reforming of methane