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Tert-butyl-λ 5 -phosphanedione was generated by flash vacuum thermolysis (FVT) of trimethylsilyl tert-butyl phosphonohalidates. The structure of tert-butyl-λ 5 -phosphanedione was confirmed by chemical reactions. Tert-butyl-λ 5 -phosphandione readily undergoes trimerization, enters into the [2 + 3] - cycloaddition reaction with 2-phenyloxirane and adds alcohols.

Generation of tert-butyl-λ 5 -phosphanedione and its chemical properties