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The vapor-phase phosphorylation of cellulose by means of phosphorus trichloride (PCl 3 ) and phosphorus oxychloride (POCl 3 ) is presented. It was found that cellulose-O-dichlorophosphines (Cell-O 6 -PCl 2 ) formed by the reaction of cellulose with PCl 3  and cellulose-O-dichloro-oxyphosphines (Cell-O 6 -P(O)Cl 2 ) formed by the reaction with P(O)Cl 3  have been hydrolyzed to cellulose-O-hydrogenphosphates (P(III/V)) (Cell-O 6 -P(O)(H)-OH and (Cell-O 6 -P(O)(OH) 2 ), respectively. Selected chemico-physical properties (SEM-EDS,  31 P NMR, potentiometric titration) of both types of cellulose phosphates (Cell-O 6 -O-P(O)(H)-OH and Cell-O 6 -O-P(O)(OH) 2 ) were compared.

Phosphorylation of the cellulose surface with PCl 3 and P(O)Cl 3