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The CAL-B-mediated kinetic resolution of racemic 2-hydroxymethylphenyl-(methyl)phenylphosphine and its  P -BH 3  analogue gave,  via  their enantioselective monoacetylation, the corresponding monoacetates and unreacted substrates in moderate yields and with indeterminate enantiomeric excess, depending on the solvent applied. The  P -BH 3  analogues were transformed into 2-aminomethyl derivatives  via O- tosyl or  O -mesyl intermediates, which will be checked as tridentate catalyst/ligands in asymmetric synthesis.

Enzymatic kinetic resolution in the synthesis of new precursors of P- chiral organophosphorus catalysts: phosphines and their P- boranes