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The Cs 2 CO 3 -promoted P-N coupling reaction of H-phosphoryl compounds and N-tosylhydrazones is reported. Formally, this transformation represents an interesting example of exchanging the sulfur and phosphorus functionalities to convert N-tosylhydrazones to N-phosphorylhydrazones. The reaction may take place via the nucleophilic interception of the in-situ generated diazo intermediates by H-phosphoryl compounds at the terminal nitrogen atom.

phosphorus, sulfur, and silicon and the related elements

Cs 2 CO 3 -promoted P-N coupling reaction of H-phosphoryl compounds with  N -tosylhydrazones to afford  N -phosphorylhydrazones via diazo intermediates