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A versatile approach of iodine mediated C3-dicarbonylation of benzo[ d ]imidazo[2,1- b ]thiazoles (IBTs) with ethylbenzene has been reported. The reaction conditions were optimized by screening in various solvents, catalysts, and oxidants. The reaction is compatible with various substrates and was successfully demonstrated to offer moderate to good yields.

Iodine Mediated Oxidative Cross-Coupling of Benzo[ d ]Imidazo[2,1- b ]Thiazoles with Ethylbenzene: An Unprecedented Approach of C3-Dicarbonylation