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In this study, a novel acidic natural surface-modified nanoclinoptilolite (NCP@SiO 3 PrHMTASO 3 H) have been designed, synthesized, and fully characterized using various analytical techniques (Fourier Transform Infrared Spectroscopy (FT-IR), X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy-Dispersive X-ray Spectroscopy (EDS), Transmission Electron Microscopy (TEM), and Thermogravimetric–Analyses (TG). In addition, NCP@SiO 3 PrHMTASO 3 H nanocatalyst have been found to catalyze effectively the multi-component synthesis of Manich base containing coumarin moiety under solvent-free condition. This novel heterogeneous catalyst is easily recycled and reused several times.

Acidic Nano Zeolite Clinoptillolite; Green and Heterogeneous Catalyst for One-Pot Multi-Component Synthesis of 3-Substituted-Amino Coumarins