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Nowadays, nanoscale materials have been widely applied in the removal of contaminants from the water system. Reduction of Cr(VI) (as a poisonous species) to Cr(III) (as a slight toxic species) was performed using CuO-Kaolin with ultrasound (US) irradiation. The CuO-Kaolin nanocomposite was synthesized via a facile co-precipitation method. Then X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscope and Energy dispersive X-ray spectroscopy analyses were performed to identify the structural features of CuO-Kaolin. The role of influential parameters for the reduction of Cr(VI) was investigated in sonocatalytic advanced oxidation system. About 89.35% of Cr(VI) was removed via US/CuO-Kaolin process after 90 min at optimum conditions (pH = 3, sonocatalyst dosage = 1 g L −1  and [Cr (VI)] 0  = 20 mg L −1 ). This outstanding result was due to the synergistic effect of the increased electron delivery to conduction band on CuO-Kaolin nanocomposite and the increased reactive surface region of nanoparticles by sonication. The presence of H 2 O 2  as an amplifier improved the removal efficiency of Cr(VI) from 89.35% to 100% after 20 min. Kinetic experimental results were well described by a pseudo-first-order kinetic model. Desorption experiments showed excellent stability of sonocatalyst during the reaction and maintenance of the catalytic activity up to 10 sequential cycles.

Facile provision of CuO-Kaolin nanocomposite for boosted sonocatalytic removal of Cr(VI) from hydrous media