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Bis -1,3-isophthalimines flanked by two side 3-aryl-5-perfluoroalkylisoxazoline or 3-aryl-5-perfluoroalkylisoxazol arms were produced and liquid crystal properties were analysed. Monotropic smectic A mesophase was found for  bis -1,3-isophthalimines containing the 3-aryl-5-perfluorooctylisoxazoline ( 8b ). Thermal behaviour was analysed and discussed by DSC, POM, DFT calculations, cohesive energy density (CED), Hildebrand solubility parameters and molecular-shape features. Notably, for long side arm perfluorooctyl  8b , the reduced value of CED is partially compensated by molecular shape of the molecules in the condensed state favouring the SmA mesophase formation.

Effect of shape and nano-segregation in Δ 2 -isoxazoline and isoxazole on the mesogenic behavior of 1,3-bis-isophthalimines