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In the present work, FeNiMnCuX (X: Co, Cr, Mo, Ti, W) high entropy alloys are successfully fabricated by mechanical alloying. After 15 h of milling, FeNiMnCu and FeNiMnCuCo alloys form a single FCC structure, while other alloys formed an FCC + BCC mixture structure. All alloys contained homogeneous distributions of Fe and Ni, while Cu was segregated. Alloys FeNiMnCuTi and FeNiMnCuW exhibited homogeneous distributions of Mn, whereas others exhibited Mn-rich islands. Except for the FeNiMnCuTi alloy, all alloys exhibited a soft magnetic behaviour. The saturation magnetisation of the base FeNiMnCu alloy was increased by adding Co and decreased by adding Cr, Mo, Ti, and W.

Alloying, phases and magnetic behaviour of mechanically alloyed FeNiMnCu-based high entropy alloys