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Titanium dioxide was prepared using titanium-based metal–organic framework (MOF) i.e., NH 2 -MIL-125(Ti) as a metal precursor. NH 2 -MIL-125(Ti) was synthesized then calcined at 400 °C, 500 °C, 550 °C, and 600 °C. The properties of NH 2 -MIL-125(Ti) and produced TiO 2  were investigated using various techniques, including powder X-ray diffraction (PXRD), Brunauer–Emmett–Teller (BET), and UV–visible diffuse reflectance spectroscopy (UV–Vis DRS). A scanning electron microscopy (SEM) was used to observe surface morphology and energy-dispersive X-ray spectroscopy (EDX) to analyze elemental composition of prepared samples. PXRD pattern confirms TiO 2  anatase phase formation when Ti-MOF was calcined up to 500 °C, whereas the formation of TiO 2  rutile phase at calcination temperature of 600 °C. The photocatalytic activities of produced TiO 2  photocatalysts were investigated for the cycloaddition reaction of CO 2  to propylene oxide.

Titania Derived from NH 2 -MIL-125(Ti) Metal–Organic Framework for Selective Photocatalytic Conversion of CO 2 to Propylene Carbonate