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Giant polyoxomolybdate Na 48 [H 496 Mo 368 O 1464 S 48 ]·ca.1000 H 2 O (Mo 368 ) is a strong candidate in materials due to its electrical properties. However, the drawbacks as instability in water and agglomeration in solid are detrimental to their readily integration into functional devices. Surface modification of Mo 368  by surfactant can protect Mo 368  in chloroform, and disperse Mo 368  clusters avoiding to direct contact with each other ,  further promote the self-assembly of surfactant-encapsulated Mo 368  hybrids into ordered porous honeycomb films. A water breath figure acts as good template for the self-assembly into porous honeycomb film at air/water interface. Varying the length of surfactant carbon chains, surfactant concentration, and supporting solution can influence the film morphology. Attributing to the embedded functional inorganic Mo 368  clusters and the pore adsorption, as-prepared porous honeycomb film is active to detect hydroquinone with the detection limit of 3.53 µM by an amperometric response method.

Honeycomb films of polyoxomolybdate-surfactant hybrids and electrochemical detection of hydroquinone