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A mononuclear compound, [Co(L1) 2 (H 2 O)]·2H 2 O ( 1 ), where L1 = N,N-bis(3,5-dichlorosalicylidene)hydrazine, was synthesized under hydrothermal conditions. Note that L1 is derived from the hydrothermal  in situ  reaction of L2 (L2 = 3,5-dichlorosalicylaldehyde thiosemicarbazone). L2 is prepared by reflux using 3,5-dichlorosalicylic aldehyde and thiosemicarbazide. Although  1  is only a mononuclear structure coordinated with L1, intermolecular hydrogen-bonded interactions between two adjacent mononuclear units creates a 1D supramolecular chain. Furthermore, it self-assembles into a fascinating 2D supramolecular layer  via π ⋅⋅⋅ π  stacking between benzene rings of adjacent chains. Hirshfeld surfaces and fingerprint maps of  1  were applied to obtain data on non-covalent interactions. Antibacterial analysis shows that  1  is a potential antibacterial material and the bacteriostasis rate is higher than that of L1 ( E. coli : 89.41% for  1 , 29.09% for L1; MRSA: 93.17% for  1 , 38.54% for L1). The solid and liquid photoluminescence properties of  1  and L1 were also investigated.

journal of coordination chemistry

An antibacterial Co(II) mononuclear compound containing N,N-bis(3,5-dichlorosalicylidene)hydrazine obtained from 3,5-dichlorosalicylaldehyde thiosemicarbazone in hydrothermal conditions