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Four new zinc(II) complexes, [ZnL 2 ] ( 1 ), [ZnL( μ2 - η1 : η1 -OAc)] n  ( 2 ), [Zn 2 L 2 (μ 1,1 -N 3 )(μ 1,3 -N 3 )] n  ( 3 ) and [ZnL( μ2 -1,5-dca)] n  ( 4 ), and a new nickel(II) complex, [Ni 2 L 2 (MeOH) 2 ( μ1,1 -N 3 ) 2 ] ( 5 ), where L is the deprotonated form of 5-bromo-(((2-(phenylamino)ethyl)imino)methyl)phenol (HL), OAc is acetate and dca is dicyanamide, were synthesized and characterized by elemental analyses, infrared and electronic spectroscopy, and single crystal X-ray determination. Complex  1  is a mononuclear zinc(II) compound, with the Zn(II) in tetrahedral coordination. Complexes  2 ,  3  and  4  are acetate, azide and dicyanamide bridged polymeric zinc(II) compounds, respectively, with the Zn(II) in distorted trigonal bipyramidal coordination. Complex  5  is an azide bridged dinuclear nickel(II) compound, with the Ni(II) ion having octahedral coordination. The compounds were evaluated for their antibacterial activities on  Bacillus subtilis ,  Staphylococcus aureus ,  Escherichia coli  and  Pseudomonas fluorescens  and antifungal activities on  Candida albicans  and  Aspergillus niger . Complexes  1  and  2  showed the most effective activity against  B. subtilis  and  E. coli , with MIC values of 1.2–4.7  μ M.

Crystal structures and antimicrobial activity of zinc(II) and nickel(II) complexes of 5-bromo-(((2-(phenylamino)ethyl)imino)methyl)phenol