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A heteronuclear Tb-Al complex ( 1 ) was obtained by pyridine-2,6-dicarboxylic acid (H 2 PDA), AlCl 3  and Tb 4 O 7  under hydrothermal condition. Single-crystal X-ray diffraction analysis reveals that  1  is an ion-pair and consists of [Al(H 2 O) 6 ] 3+  cation and [Tb(PDA) 3 ] 3-  anion; the [Al(H 2 O) 6 ] 3+  cations and [Tb(PDA) 3 ] 3-  anions are further connected by hydrogen bonds to construct a 3D NaCl-like topology. Lattice water molecules in  1  fabricate a cubic (H 2 O) 8 -octamer by hydrogen bonds, which is located in the void of  1 . Luminescent property indicates efficient energy transfer from PDA 3-  ligand to Tb 3+  in  1 , exhibiting the typical green emission of Tb 3+  in the visible region.

A luminescent heterometallic Tb–Al ion-pair complex with a cubic (H 2 O) 8 -octamer