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In the present work, we report a detailed investigation of four supramolecular coordination complexes, Zn(Quino) 2 (CH 3 OH) 22 , Zn(Quino) 2 H 2 O  3 , Mn(Quino) 2 (CH 3 OH) 24  and Ca(Quino) 2 (CH 3 OH) 25 , obtained from the self-assembling of Zn(II), Mn(II) and Ca(II) acceptors with the  N -phenyl-4-hydroxyquinoline ligand donor QuinoH  1 , possessing the β,β′ - diketonate moiety. The structure of the supramolecular arrangement of the isolated complexes have been investigated by single crystal X-ray crystallography. The synthetic  N -phenyl quinolone-linker that forms a π–π stacking supramolecular synthon with the coordination preferences of metal ions has been used to construct coordination driven self-assembled “metallosupramolecular” architectures.

Synthesis and structural studies of quinolone-based Zn(II), Mn(II) and Ca(II) complexes involving supramolecular interactions