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Two three-dimensional (3D) nickel-based metal-organic frameworks (Ni(II)-MOFs), {[Ni(adc)(phen)(H 2 O)]} n  ( 1 , H 2 adc = 9,10-anthracenedicarboxylic acid, phen = 1,10-phenanthroline) and {[Ni(adc)(bpy)]} n  ( 2 , bpy = 4,4’-bipyridine), were synthesized via a mixed-ligand strategy under hydrothermal and solvothermal conditions. MOF  1  could be simplified as a binodaltfctopology, while  2  possesses a three-fold interpenetrated framework, which is composed of a 4-connecteddianetwork. The phase purity, molecular vibrations, and thermal stability of  1  and  2  have been characterized by powder X-ray diffraction (PXRD), infrared spectroscopy (IR), and thermogravimetric analysis (TG). Further electrochemical experiments reveal that  1  and  2  exhibit good methanol/ethanol oxidation (MOR/EOR) activities, with the optimal current density reaching up to 21.2 (EOR: 25.3) and 15.8 (EOR: 15.3) mA cm −2 , respectively.

Synthesis, characterization and crystal structure of two nickel-based metal-organic frameworks with electrocatalytic activity