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Atomically precise Ag-doped polyoxo-titanium oxo clusters (Ag-PTCs) are beneficial for the investigation on structure-property relationship of silver doped TiO 2  materials. Although several Ag-PTC clusters have been reported, their hierarchical assembly into multidimensional structures remains unexplored. In this work, di-phosphine ligands with various carbon chain lengths were exploited to stabilize and induce the hierarchical assembly of Ti 8 Ag 2  oxo clusters. Correspondingly,  cis-  and  trans -isomers of {Ti 8 Ag 2 } are generated in the discrete cluster ( PTC-337 ) and two 1D-chains ( PTC-338  and  PTC-339 ), respectively. Light absorption behaviors of the obtained compounds were also studied.

Hierarchical assembly and structural regulation of Ti 8 Ag 2 oxo clusters via varying the length of the carbon chains in di-phosphine ligands