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Two new Cu(II) complexes, {CuL 2 ⋅(4,4′-bipy)} n  ( 1 ) and CuL 2 (Py) 2  ( 2 ), where bipy = bipyridine; HL = N-(bis(diethylamino)phosphoryl)-2,2,2-trichloroacetamide, representative of carbacylamidophosphate (CAPh) type ligands), have been synthesized and characterized by FTIR and single-crystal X-ray analysis. In both complexes CAPh ligands are coordinated to the copper ions in a bidentate chelate manner through oxygens of the carbonyl and phosphoryl groups. Nitrogen atoms of bipyridine,  1 , or pyridine molecules,  2 , complete the coordination number of Cu(II) to six. The Cu ions are located in special positions on inversion centers. In the structure of  1 , the bipyridine molecules display a bridging function between adjacent copper complexes forming a polymer chain. Phosphoryl and 4,4′-bipy (Py) ligands in both structures are located in  trans  positions relative to each other.

Copper(II) complexes based on N-(bis(diethylamino)phosphoryl)-2,2,2-trichloroacetamide with pyridine and 4,4′-bipyridine