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An I 2 -mediated  N – N  coupling reaction has been described for oxidation cyclization of 2,2,2-trifluoro- N -(1-iminoethyl)- N ′-arylacetimidamide to synthesis of novel 3-methyl-1-aryl-5-(trifluoromethyl)-1 H -1,2,4-triazole derivatives under mild conditions with excellent yield without need to any purification. This procedure doesn’t have need to use of transition metals an also, can be used on gram scale. This synthetic method does not require use of transition metals and can be conveniently carried out on gram scale.

2,2,2-Trifluoro- N -(1-iminoethyl)- N ′ arylacetimidamides as key intermediate for synthesis of trifluoromethyl 1,2,4-triazoles