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Highly regiospecific  ortho –nitration of electronically diverse phenols is accomplished using Fe(NO 3 ) 3 .9H 2 O for electron–rich and Cu(NO 3 ) 2 .6H 2 O for electron–deficient phenols as the cheap nitrating agents. The reaction is carried out in CH 3 CN at 90 °C under mild and neutral conditions where structurally diverse phenols afford exclusively  ortho –nitration products in moderate to good yields with outstanding tolerance of functional groups. The synthetic application of this strategy was established by achieving the bioactive compound nitroxynil.

Metal nitrate promoted highly regiospecific ortho –nitration of phenols: Application to the synthesis of nitroxynil