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Nitration of  N -acetyl anilides using a simple combination of AgNO 3  and K 2 S 2 O 8  as a stable nitro source and an oxidant, respectively, was explored. The reaction was practical to operate and proceeded under considerably mild reaction conditions (reflux in acetonitrile) within acceptable reaction time (6 h). The  para -substituted  N -acetyl anilides gave only  ortho -nitrated products in moderate to good yields (30–63% yields). The  ortho -,  meta -, or non-substituted  N -acetyl anilides gave a mixture of nitrated products (30–72% combined yields) with preferentially at the  para - over the  ortho -position ( ortho : para ; 1.0:1.1–1.0:2.8).

Nitration of N -acetyl anilides using silver(I) nitrate/persulfate combination