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We have developed a highly atom efficient synthesis of tetrasubstituted 3(2 H )-furanones from easily accessible starting materials such as  C,N -diarylaldonitrones and dibenzoylacetylene. Control experiments revealed that reaction of aldonitrones having electron-withdrawing groups on the  C -aryl substituent in polar aprotic solvents exhibited high product selectivity while reaction temperature has only a negligible effect on product yield and selectivity.

Highly atom efficient synthesis of 2,2,4,5-tetrasubstituted 3(2 H )-furanones having both hydroxyl and amino substituents