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A pseudo-five-component reaction leading to efficient synthesis of dicyanoanillines was developed using only aromatic aldehydes and malononitrile as the starting reactants. Mechanistic studies suggested that a malononitrile dimer and the Knoevenagel condensation product of benzaldehyde, initially formed in the reaction mixture, combine with a fourth equivalent of malononitrile to form the final product. X-ray crystallography analysis of one of the derivatives confirmed the structure of the products.

Pseudo-five-component organocatalyzed synthesis of dicyanoanillines using only malononitrile and aromatic aldehydes