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Direct carbon–carbon bond scissions enable the utilization of hydrocarbons in efficient manners and therefore attract much current interest. In this review we summarize the transition metal mediated aromatic hydrocarbons C(sp 3 )–C(sp 2 ) bond activation processes. In the first part, we introduce the C(sp 3 )–C(sp 2 ) bond scission via either transition metals insertion into the C–H bond followed by C–C activation or transition metals direct insertion into the C–C bond. In the second part, C(sp 3 )–C(sp 2 ) bond cleaving transformations using transition metal such as iron and copper as a single-electron-transfer (SET) catalyst for the oxidative scissions was outlined.

Transition metal mediated activation of C(sp 3 )–C(sp 2 ) bond in aromatic hydrocarbons