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In this research, the effects of calcination temperature in a range of 1050–1200 °C for 2 h and sintering temperature in a range of 1325-1400 °C for 2 h on phase formation, microstructure and electrical properties of lead-free Ba 0.9 Ca 0.1 TiO 3  (BCT) ceramics fabricated via the solid-state combustion technique were investigated. For the XRD result, all the ceramics exhibited a coexisting phase between tetragonal and orthorhombic. The ceramic grain size tended to increase with increase of the sintering temperature. For BCT ceramic produced by the optimum sintering temperature (1375 °C for 2 h), the dielectric, ferroelectric and piezoelectric properties of  εC =7393,  Pr =7.60 μC/cm 2,EC =5.99 kV/cm and  d33 =158 pC/N, respectively, were obtained.

Phase formation, microstructure and electrical properties of Ba 0.9 Ca 0.1 TiO 3 ceramics fabricated via the solid-state combustion technique