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The number of spent batteries has increased significantly in recent years due to the use of mobile phones, vehicles, and other high-tech products. In this work, the vitroceramics of the  x Sb 2 O 3 ·5MnO 2 ·(95- x )[9Pb·PbO 2 ] composition where  x  = 0 − 40 mol% Sb 2 O 3 , were synthesized by melt-quenching method using as raw materials the spent plates of a car battery (the anode as the Pb source and the cathode as the PbO 2  source), MnO 2  and Sb 2 O 3  powders. The prepared samples were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, ultraviolet–visible spectroscopy, and cyclic voltammetry. The electrochemical performance of the antimony–manganese–lead materials used as working electrodes for a car battery were demonstrated by cyclic voltammetry. The combined results from various techniques show that the antimony ions play an important role in the conductive and electrochemical properties.

Manganese Dioxide–Antimony Trioxide–Lead–Lead Dioxide Vitroceramics Obtained from Recycled Lead Acid Batteries