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Significance This work reveals that Fe4+δ Se5 with ordered Fe vacancy is a nonoxide compound with the Verwey-like electronic correlation. Detailed measurements showing magnetic field-independent magnetoresistance at low temperature suggest it is in a charge-ordered state belowT ≈ 17 K. The results of the field orientation measurements indicate that the spin-orbital coupling is crucial in √5 × √5 Fe vacancy-ordered Fe4+δ Se5 at low temperatures. Our findings provide valuable information to better understand the orbital nature and the interplay between the metal-insulator transition and superconductivity in FeSe-based materials.

Magnetotransport studies of Fe vacancy-ordered Fe 4+δ Se 5 nanowires

Magnetotransport studies of Fe vacancy-ordered Fe _4+δ Se ₅ nanowires