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Significance The electrocatalytic conversion of CO2 to value-added products, especially valuable multicarbon products, is a pathway toward sustainable formation of chemicals and fuels typically derived from fossil fuels, while mitigating CO2 emissions. Fundamental understanding and development of more efficient catalysts for this reaction require deep investigation into structures with high intrinsic activity, which are limited at present. This work comprehensively investigates a dynamic copper nanoparticle ensemble catalyst that significantly improves intrinsic activity of copper for multicarbon formation. Through concerted ex situ and in situ characterization techniques, it illustrates an electrochemically induced fusion of copper nanoparticles that result in a catalytically active disordered structure, motivating closer study of disordered metal nanostructures for C–C coupling electrocatalysis.

Electrochemically scrambled nanocrystals are catalytically active for CO 2 -to-multicarbons

Electrochemically scrambled nanocrystals are catalytically active for CO ₂ -to-multicarbons