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Significance Oxidation and reduction steps in catalysis are always in series, and excellent activity can be achieved when they occur in close proximity. Photooxidation and photoreduction are generally separated and rarely in series. This work develops defect engineering at the metal–oxide interface to make photooxidation sites close to photoreduction sites. Taking solar hydrogen production from aqueous alcohols over Pt/T i O 2 as an example, the proximity effect triggers unusual reactions and thus increases hydrogen yield per photon from 0.046 to 1.28. Our study provides a direction for the development of efficient photocatalysis.

Defect engineering of metal–oxide interface for proximity of photooxidation and photoreduction