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Analysis by tritium n.m.r, of triethylsilane, tetramethylsilane, hexamethyldisiloxane and chlorodimethylsilane exchanged with tritium gas over Raney nickel at 100°C shows that exchange readily occurs in alkyl substituents as well as with silyl hydrogen; novel species involving charge-transfer intermediates in dissociative adsorption at the C-H as well as the Si-H bonds are proposed to explain the data.

Metal-catalysed exchange of alkyl and silyl hydrogen in organosilanes with tritium gas over Raney nickel as measured by 3H N.M.R