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A comparison of theasymmetric stretching frequency v3 and unit cell length a0for a series of hexahalogeno-metallates A2MX6[A = K+, Rb+, Cs+and NH4+, M = Ru, Os, Sn and Teand X = Cl,Br] has been made. Trends observed for thetellurium and tin compounds may be related to stericfactors whereas possible M →X dπ-pπ bonding mayexplain the opposite trend found for ruthenium and osmium compounds.

The influence of π-bonding and steric factors on helahalogeno-metallates