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The presence of small amounts of ferric chloride1 has been found to adversely affect current efficiencies during electrodeposition of metals from molten chlorides. Suggestions are that this is due to the anodic oxidation of Fez+ and cathodic reduction of Fe3+ dissolved in the melts. Ferrous compounds could also be oxidized by anodically evolved chlorine which dissolves in chloride melts.2 Besides influencing current efficiencies small amounts of iron co-deposited have been found to have adverse effects on the nature of the co-dep~si t .~ Iron compounds are often present in bulk quantities of chloride due to the method of manufacture and are difficult to remove by normal laboratory purification method^.^,^ In this work co-deposition was found to be unsatisfactory; however, oxidation by bubbling oxygen through the melt quantitatively removed all iron from the solution.

The removal of dissolved iron chlorides from molten chloride mixtures