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The influence of thermal disorder and static distortions on the localstructure in microcrystalline solid solutions of tungstates ZncNi1-cWO4 withc=0.0-1.0 was investigated using temperature-dependent (10-300 K) x-rayabsorption spectroscopy (XAS) at the W L3-edge. In addition, the vibrationalproperties of the solid solutions were studied by Raman spectroscopy. Ourresults indicate that the formation of solid solutions is accompanied by strongstructural relaxations leading to the changes in the [WO6] octahedradistortions, which, in turn, affect the vibrational properties of tungstates.In particular, the frequency and band width of the highest W-O stretching modeat about 900 cm-1 show distinct composition dependence, following the localstructure modifications as revealed by XAS.

X-ray absorption and Raman spectroscopy studies of tungstates solid solutions ZncNi1-cWO4 (c=0.0-1.0)