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The nanoparticles (NPs) of Zn1-xCuxFe2O4 (ZCFO) spinels with x = 0, 0.2, 0.4,0.6 and 0.8 were synthesized by a sol-gel combustion method using acetateprecursor. The NPs of ZCFO were prepared by following calcination process at600C for 8hrs. The synthesized NPs of ZCFO were characterized by X-raydiffraction (XRD) analysis using Rietveld refinement. The Rietveld refinementof the XRD patterns revealed that the ZCFO spinels crystallize into singlediamond cubic structure with Fd-3m space group. The lattice constant and unitcell volume for ZCFO NPs shrink with enhancing doping concentration of Cu2+ion. The crystalline growth in the NPs of ZCFO was examined by peak broadeningpresent in the XRD pattern. The Williamson-Hall (W-H) plot method were used tostudy the individual involvements of crystallite sizes and lattice strain onthe peak broadening of the NPs of ZCFO spinels. Whereas, particle size of theZCFO sample with x = 0.40 was estimated by high-resolution scanning electronmicroscopy micrographs

X-ray Diffraction Analysis of Cu2+ Doped Zn1-xCuxFe2O4 Spinel Nanoparticles using Williamson-Hall Plot Method