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We report on the observation of rich variety of crystallographic phaseformation in RexMo1-xS2 alloy for x < 0.5. For x < 0.23, no low dimensionalsuper-structural modulation is observed and inter-cation hybridization remainsdiscrete forming dimers to tetramers with increasing Re concentration. For x >0.23, super-strutural modulaton is observed. Depending on the Re concentrations(x = 0.23, 0.32, 0.38 and 0.45) and its distributions, various types of cationhybridization results in rich variety of low dimensional super-structuralmodulation as directly revealed by high resolution transmission electronmicroscopy. These layered alloy system may be useful for various energy andnovel device applications.

Rich diversity of crystallographic phase formation in 2D Rex:Mo1-xS2 (x< 0.5) alloy