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The structural evolution of Co40Fe22 Ta 8B30 glassy particles has been studied by in-situ high-energy synchrotron X-ray diffraction (XRD) upon isochronal annealing. The changes in position, intensity, and full width at half maximum (FWHM) of the first and second diffuse maxima of the XRD patterns suggest the occurrence of irreversible structural relaxation upon the first heating up to a temperature close to the glass transition temperature Tg . The variations in reduced pair correlation functions upon annealing are discussed in the frame of the topological fluctuation theory for structural relaxation. Isochronal annealing of the Co40Fe22 Ta 8B30 glassy particles improves their soft magnetic properties through decreasing the coercivity and increasing the magnetic susceptibility, saturation magnetization, and Curie temperature

Thermal and soft magnetic properties of Co40Fe22Ta8B30 glassy particles: In-situ X-ray diffraction and magnetometry studies