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Antiphase domains are seen in single crystal gamma lithium aluminate (γ-LiAlO2) with 16.7 nm periodicity in the ⟨110⟩ direction. Alternate domains have a 12 [001] shift. Beta phase lithium aluminate (β-LiAlO2) is seen to form on the surface of the as-received wafers with an epitaxial strain limited relationship with the bulk γ phase. The orthorhombic β phase aligns with the a and b axes (0.528 and 0.630 nm) matching with the tetragonal γ phase’s a and c axes (0.5168 and 0.6268 nm). The γ and β phases are seen to have different etch rates. The β phase converts back to the γ phase above 450 °C.

Antiphase ordering and surface phases in lithium aluminate