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Single-phase bulk samples of the "exotic" CoO2, the x = 0 phase of the AxCoO2systems (A = Li, Na), were successfully synthesized through electrochemicalde-intercalation of Li from pristine LiCoO2 samples. The samples of pure CoO2were found to be essentially oxygen stoichiometric and possess a hexagonalstructure consisting of stacked triangular-lattice CoO2 layers only. Themagnetism of CoO2 is featured with a temperature-independent susceptibility ofthe magnitude of 10-3 emu/mol Oe, being essentially identical to that of aLi-doped phase, Li0.12CoO2. It is most likely that the CoO2 phase is aPauli-paramagnetic metal with itinerant electrons.

Electrochemical synthesis and properties of CoO2, the x = 0 phase of the AxCoO2 systems (A = Li, Na)