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Results of Rietveld analysis of the synchrotron XRD data on Pb(Zr_xTi_1-x)O_3(PZT) for 0.525\leqx\leq0.60 are presented to show the absence of rhombohedralphase on the Zr-rich side of the morphotropic phase boundary (MPB). Our resultsreveal that the structure of PZT is monoclinic in the Cm space group for0.525\leq x\leq 0.60. The nature of the monoclinic distortion changes frompseudo-tetragonal for 0.525\leqx\leq0.54 to pseudo-rhombohedral for x>0.54.

applied physics letters

High-resolution synchrotron XRD study of Zr-rich compositions of  Pb(Zr_xTi_1-x)O_3 (0.525\leq x \leq 0.60): evidence for the absence of the  rhombohedral phase