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Solid-state NMR technique for measureing distances between hetero-nuclei instatic powder samples is described. It is based on a two-dimensionalsingle-echo scheme enhanced with adiabatic cross-polarization. As an example,the results for intra-molecular distances in $\alpha$-crystalline form ofglycine are presented. The measured NMR distances ^13 C(2) - ^15 N and ^13 C(1)- ^15 N are 1.496 $\pm$ 0.002 \AA and 2.50 $\pm$ 0.02 \AA, respectively.Comment: 12 page

Accurate measurement of C13–N15 distances with solid-state NMR