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We report a method that allows direct, systematic, and accurate determination of the atomic structure of multiwalled carbon nanotubes by analyzing the scattering intensities on the nonequatorial layer lines in the electron diffraction pattern. Complete structure determination of a quadruple-walled carbon nanotube is described as an example, and it was found that the intertubular distance varied from 0.36nmto0.5nm with a mean value of 0.42nm.

Accurate determination of atomic structure of multiwalled carbon nanotubes by nondestructive nanobeam electron diffraction