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The first copper-catalyzed cyanation through alkene C–H bond activation by using an α-iminonitrile as a cyanating agent has been realized. The approach efficiently constructs acrylonitriles in good yields with the advantages of high regioselectivity, cost-benefit, and operational simplicity.

Copper-Catalyzed C–H Stereoselective Cyanation of Alkenes by Using an α-Iminonitrile as a Cyanating Reagent