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Mössbauer spectra of FeCl3, vapour deposited at low temperatures, show two quadrupole doublets above 6.5 K and magnetic hyperfine splittings below 6.5 K. Upon heating to 300 K the samples can be transformed irreversibly to the normal crystalline phase. Below their magnetic transition temperatures the spectra of both vapour quenched phases and of the normal crystalline phase exhibit relaxation effects which are interpreted as superparamagnetic fluctuations. In contrast to the amorphous ferrous halides, the magnetization curves of the vapour quenched phases of FeCl3 show the same functional dependence as the crystalline phase. It is suggested that the low temperature deposition of FeCl3 leads to microcrystalline rather than to amorphous structures

LOW TEMPERATURE PHASES OF MICROCRYSTALLINE FeCl3

LOW TEMPERATURE PHASES OF MICROCRYSTALLINE FeCl₃