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One-pot synthesis of polyaniline/Fe 3 O 4  nanocomposite in 1-methyl-3-alkylcarboxylic acid imidazolium chloride ([CMMIm]Cl) ionic liquid (IL) was introduced for the first time in this work. Transmission electron microscopy (TEM), X-ray diffraction (XRD), four probes method and vibrating sample magnetometer (VSM) were used to explore the influence of IL on the structure, conductivity and magnetic properties of polyaniline/Fe 3 O 4  composite. Compared with Fe 3 O 4  particles prepared in water, the results show that Fe 3 O 4  particles prepare in imidazolium-based ionic liquid were more regular in shape and dispersed uniformly. So the Fe 3 O 4  nanoparticles prepared in IL can easier serve as cores to form the polyaniline/Fe 3 O 4  nanocomposite via in situ chemical oxidative polymerization of aniline molecule. The saturation magnetization of polyaniline/Fe 3 O 4  nanocomposite prepared in ionic liquid shows about 2 times higher than polyaniline/Fe 3 O 4  composite prepared in water. And the conductivities of PANI/Fe 3 O 4  composite prepared in IL decreased and the saturated magnetization increased with the increasing amount of Fe 3 O 4 .

One-pot synthesis of polyaniline/Fe3O4 nanocomposite in ionicliquid: electrical conductivity and magnetic studies

One-pot synthesis of polyaniline/Fe₃O₄ nanocomposite in ionicliquid: electrical conductivity and magnetic studies